Volumetric Hydrogen Sorption Measurements − Uncertainty error analysis and the importance of thermal equilibration time

Simple item page
dc.contributor.authorDemirocak, Dervis Emre
dc.contributor.authorRam, M. K.
dc.contributor.authorSrinivasan, S. S.
dc.contributor.authorGoswami, D. Y.
dc.contributor.authorStefanakos, E. K.
dc.date.accessioned2019-10-22T15:43:26Z
dc.date.available2019-10-22T15:43:26Z
dc.date.issued2013-02-06
dc.description.abstractAbstract The design of a volumetric measurement apparatus is studied by means of an uncertainty analysis to provide guidelines for optimum hydrogen sorption measurements. The reservoir volume should be as small as possible (i.e., 10 cc) to minimize the uncertainty. In addition, the sample mass loading has a profound effect on the uncertainty and the optimum loading is a function of the sample's intrinsic storage capacity. In general, the higher the sample mass loading the lower the uncertainty, regardless of any other parameter. In cases where the material to be tested is not available in gram quantities, the use of high accuracy pressure and temperature transducers significantly mitigates the uncertainty in the sample's hydrogen uptake. Above all, the thermal equilibration time is an important parameter for high accuracy measurements and needs to be taken into consideration at the start of the measurements. Based on a computational analysis, a 5 min wait time is required for achieving thermal equilibrium when the instrument enclosure temperature is different than the ambient temperature.en_US
dc.identifier.citationDE Demirocak, SS Srinivasan, MK Ram, DY Goswami & EK Stefanakos, Volumetric Hydrogen Sorption Measurements − Uncertainty error analysis and the importance of thermal equilibration time, International Journal of Hydrogen Energy, 2013, 38, 1469–77.en_US
dc.identifier.urihttps://hdl.handle.net/10657.1/1601
dc.relation.ispartofseriesInternational Journal of Hydrogen Energy;Vol. 38, Issue 3, pp. 1469-1477
dc.titleVolumetric Hydrogen Sorption Measurements − Uncertainty error analysis and the importance of thermal equilibration timeen_US

Files

Original bundle

Now showing 1 - 1 of 1
Thumbnail Image
Name:
Volumetric Hydrogen Sorption Measurements − Uncertainty error analysis and the importance of thermal equilibration time.pdf
Size:
330.75 KB
Format:
Adobe Portable Document Format
Description:
Download

License bundle

Now showing 1 - 1 of 1
No Thumbnail Available
Name:
license.txt
Size:
1.71 KB
Format:
Item-specific license agreed upon to submission
Description:
Download

Collections

College of Science and Engineering